Natural food ingredients from quince peel: Towards a "zero-waste" production system
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Quince is the yellow fruit of the deciduous tree Cydonia oblonga Mill. Its taste is sour and astringent when eaten raw,
so it is usually processed into marmalade and many other food products, mostly sweets, through processes that
discard the peel as a by-product. Therefore, this work was carried out to promote the upcycling of quince peel into
valuable food ingredients following a "zero waste" approach. A response surface methodology (RSM)-coupled
experimental design with 20 runs, combining five levels of time (1–120 min), temperature (25–95 °C) and ethanol
concentration (0–100%), was implemented for maximizing the extraction of soluble solids and malic acid while
simultaneously obtaining fiber concentrate extracts. The yields of soluble solids and fiber concentrate extracts were
determined gravimetrically. Malic acid, which has been used as a food preservative, was analyzed by ultra-fast liquid
chromatography with photodiode array detection.1 The dietary fiber content of the fiber concentrate extracts was
determined by an enzymatic-gravimetric method (AOAC Official Method 985.29) and their color was measured with
a portable colorimeter.2,3 The three independent variables affected significantly the extraction process and the
predictive model equations were validated based on different statistical criteria, which allowed to determine the
optimal extraction conditions. In general, the soluble solids yield was promoted by lower temperatures and ethanol
concentrations, while malic acid was better extracted at higher temperatures for longer processing times. In turn, the
fiber concentrate extracts remaining after extraction had opposite yields to the soluble solids. However, the highest
yields of these fiber concentrates were not in agreement with their dietary fiber contents. The highest fiber values
were recorded in the concentrate extracts obtained at high temperatures and medium-low ethanol concentrations.
In fact, only these two independent variables significantly impacted its extraction, through linear, quadratic, and also
interactive effects. Furthermore, the lighter fiber concentrate extracts were those with the highest yields. Overall,
quince peel can be totally upcycled into natural food ingredients rich in malic acid and dietary fiber.
The resources on our planet are finite and limited. Nonetheless,
more and more waste is being produced worldwide. In this sense, it
is essential to acquire circularity and "zero waste" approaches to
move from the current environmentally unsustainable agri-food
system to a more sustainable practice. Quince is the yellow fruit of
the deciduous tree Cydonia oblonga Mill. This fruit has an intense
aroma, flavor and acidity, but most varieties are too sour and
astringent to be eaten raw, so it is usually processed into marmalade
and many other food products, mostly sweets, through processes
that discard the peel as a by-product. Therefore, this work was
carried out to promote the upcycling of quince peel into valuable
food ingredients following a "zero waste" approach. Thus, it was
intended to optimize the extraction of compounds of interest to the
food industry using the response surface methodology (RSM).